HITACHI S-4800 FIELD EMISSION SCANNING ELECTRON MICROSCOPE (FE-SEM)

Location: Egan Research Center, Room 106

Status: Operational

Booking: Priority Software® FBS

Description: Hitachi S-4800 FE-SEM is a high-resolution scanning electron microscope (SEM) with cold field emission gun. It is equipped with the energy-dispersive X-ray spectroscopy (EDS) system (EDAX detector and Team software) that enables elemental analysis. It also has a Nabity nanolithography e-beam pattern generation system.

Instrument Specifications:

Electron SourceCold Field Emission Gun
Accelerating Voltage500V to 30kV in 100V steps
Resolution1.0 nm Accelerating Voltage 15kV, Working Distance 4 mm
2.0 nm Accelerating Voltage 1kV, Working Distance 1.5 mm
MagnificationHigh Mag Mode 100x to 800,000x
Low Mag Mode 30x to 2,000x
Specimen StageX Traverse 0 to 110 mm
Y Traverse 0 to 110 mm
Z Traverse 1.5 to 40 mm
Tilt -5° to +70°
Rotation 360°
Specimen SizeMax. 150 mm (6″)
Image ModeSecondary Electron Imaging
Back Scattering Electron Imaging
AccessoriesEDAX system with Teams software

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TESCAN VEGA 3 LMU VARIABLE PRESSURE SCANNING ELECTRON MICROSCOPE (VP-SEM)

Location: Egan Research Center, Room 429

Status: Operational

Booking: Priority Software® FBS

Description: TESCAN VEGA 3 LMU variable pressure scanning electron microscope (VP-SEM) has a thermionic-W electron source and suitable for imaging solid or semi-liquid samples.  It is equipped with an Oxford energy dispersive spectrometer (EDS) for sub-micron spatial resolution elemental analysis and an Oxford electron backscatter diffraction (EBSD) system for in situ mineralogical and crystallographic analysis of biomineralized structures. The system also supports rapid mapping of elemental composition and crystallographic orientations.

Electron SourceTungsten heated cathode
Accelerating Voltage200 eV to 30 keV
ResolutionHigh Vacuum Mode (SE):
3 nm at 30 kV / 2 nm at 30 kV
8 nm at 3 kV / 5 nm at 3 kV

Low Vacuum Mode (BSE, LVSTD):
3.5 nm at 30 kV / 2.5 nm at 30 kV
Magnification2x – 1,000,000x
(for 5’’ image width in Continual Wide Field/Resolution)
Specimen StageType: Compucentric, fully motorized
Movements:
X = 80 mm (–40 mm to +40 mm)
Y = 60 mm (–30 mm to +30 mm)
Z = 47 mm
Rotation: 360° continuous
Tilt: –80° to +80°
Maximum Specimen Height:
54 mm (with rotation stage)
81 mm (without rotation stage)
Probe Current1 pA to 2 uA
Image ModeResolution: High-resolution mode
Depth: Sets the column up in a mode that enhances depth of focus
Field: Optimizes the column to provide a large non-distorted field of view
Wide Field: Provides an extra-large non-distorted field of view for extra low
magnification imaging
Channeling: Working mode for assessment of crystal orientation data of the specimen,
acquiring of electron channeling pattern (ECP)
AccessoriesOXFORD EDS & EBSD systems with Aztec software